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Given this situation, the rational control of the crystal structure of an alloy system is also very attractive and challenging.
Here, we propose an approach for the selective control of the crystal structure of solid-solution alloys at a certain composition using the chemical reduction method.
The crystal structure of binary alloy NPs could be dominated by the structure of the nuclei that are formed from one of the constituent metal ions, which start to be reduced slightly earlier than the other during the alloy formation process.
By finely tuning the reduction speed of the metal precursors, which is one of the advantages of the chemical reduction method, we achieve the selective control of the crystal structure.
The temperature of the solution was maintained at 190 °C during the dropping process.
The NPs were separated by centrifuging after cooling to room temperature, as denoted by the fcc-Au Ru and CTAB were dissolved in DEG in a 1: molar ratio.
The structures of the obtained NPs are investigated using synchrotron powder X-ray diffraction (XRD) analysis and atomic resolution scanning transmission electron microscopy (STEM).
In addition, we discuss the mechanism of crystal structure control using the results of ultraviolet–visible (UV–vis) spectral and electrochemical analyses.
A solid-solution alloy, in which the constituents are randomly mixed at the atomic scale, generally adopts one of three principal crystal lattice forms: body-centred cubic (bcc), hexagonal close-packed (hcp) and face-centred cubic (fcc) structures.
However, once its constituent element and composition are fixed, the crystal structure of solid-solution alloy is uniquely determined.
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